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Trial Number 1

Trial Purpose:

To evaluate selected cleaners for the removal of epoxy resin and rubber gasket.

Date Run:

03/22/2001

Experiment Procedure:

Three products were selected for evaluation. All three were used at full strength and room temperature. A 500 ml beaker was filled with each solution. One part with gasket was immersed in the beaker. Observations were made at 5 minutes, 2, 3 and 4 hours. At each observation time, the part was removed from the beaker. The rubber gasket was checked for swelling and was removed when the gasket was easily separated from the potting fixture. The epoxy resin was wiped with a paper towel to determine if any epoxy could be removed.
SUBSTRATE MATERIAL: Potting fixture (Deiron plastic)
CONTAMINANTS: Emerson & Cuming Stycast 1090 Black, epoxy resin (DGEBA 1675-54-3, Carbon black 1333-86-4)

Trial Results:

Both Bio T Max and the D-limonene caused swelling of the rubber gasket after the first five minutes of soaking.  The Ionox HC 2 required four hours for easy removal of the gasket.  The epoxy was removed from the parts soaked in the Bio T Max after 4 hours of soaking.  The resin was pealed off in one piece.  The D-limonene did not remove the epoxy even after soaking overnight.  Ionox HC 2 was successful in removing the epoxy after two hours.  Table 2 lists the observations made at each time interval.

 

Product

 

5 min

 

2 hours

 

3 hours

 

4 hours

 

Overnight

 

Bio T Max

 

Swelling of ring-

removed

 

Some removal of epoxy (flakes)

 

Some removal of epoxy (flakes)

 

Removal of epoxy (one piece)

 

N/A

 

Ionox HC 2

 

No swelling of ring

flecks of epoxy removed

 

No swelling of ring

Removal of epoxy (one piece)

 

Starting to swell

 

Ring removed

 

N/A

 

D-Limonene

 

Swelling of ring-removed

 

Some removal of epoxy (flakes)

 

Some removal of epoxy (flakes)

 

Bigger pieces removed

 

No complete removal of epoxy

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

The two products from the previous trials, Bio T Max and Ionox HC 2, were successful in removing the rubber gasket and the epoxy resin within 4 hours of soaking.

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