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Trial Number 22

Client Number 108

Project Number 1

Trial Purpose:

To qualify the proposed cleaning method to current process and laboratory system.

Date Run:

02/17/2000

Experiment Procedure:

Laboratory baseline evaluation was performed using a 0.5% solution made up of the cleaner and DI water in the ultrasonic tank (total volume of solution was approximately 16 liters). The solution was heated to 110 F.

Thirteen coupons were cleaned in Micro 90 at 0.5% using ultrasonic energy for 10 minutes. The coupons were weighed to establish a baseline level of cleanliness.
The coupons were coated with the Evanol and dried for ten minutes at room temperature and then for 20 minutes at 212 F in an oven. All thirteen coupons were placed in a holder and submersed in the solution. Cleaning was performed in the solutions for five minutes using ultrasonic cleaning at 40 kHz using a Crest ultrasonic tank model 4Ht 1014-6. Two stage rinsing was used. The first rinse was for two minutes in DI water at 110 F and the second was for one minute at the same temperature. The parts were dried in a convection oven at 212 F for 20 minutes. After allowing parts to cool to room temperature, final weights were recorded.
The other two cleaning systems were performed off site. All coupons were weighed and contaminated at the laboratory using a Denver Instrument Co Analytical Balance model A-250.

SUBSTRATE MATERIAL: Ceramic-Alumina coupons
CONTAMINANTS: DuPont Evanol Concentrated (Vinyl Alcohol Polymers & Copolymers CAS#s: 9002-89-5, 25213-24-5, 54626-91-4; Methanol Bulk/Packaged CAS #: 67-56-1; Sodium Acetate CAS#: 127-09-3)

Trial Results:

The new cleaning system performed as well as the old system and better than the laboratory model. Table 1 lists the calculated efficiencies for each coupon cleaned using the proposed system. Table 2 compares the results from the three systems.

Table 1. New Process Efficiency

C #  Initial wt Cont wt Clean wt wt cont  Final cont % Removed
14 5.9823 6.0601 5.9824 0.0778 0.0001 99.87
15 5.9969 6.0963 5.9969 0.0994 0.0000 100.00
16 5.9921 6.0089 5.9917 0.01679 -0.0004 102.38
17 6.0073 6.1175 6.0072 0.1102 -0.0001 100.09
18 5.9688 6.0427 5.9682 0.0739 -0.0006 100.81
19 6.0076 6.088 6.0073 0.0804 -0.0003 100.37
20 5.9935 6.0578 5.9936 0.0643 0.0001 99.84
21 5.9878 6.0722 5.9877 0.0844 -0.0001 100.12
21 5.9948 6.0868 5.9945 0.092 -0.0003 100.33
23 5.9527 6.0202 5.9526 0.0675 -0.0001 100.15
24 5.9584 6.0478 5.9584 0.0894 0.0000 100.00
25 5.9896 6.0774 5.9898 0.0878 0.0002 99.77
26 5.9847 6.0763 5.9848 0.0916 0.0001 99.89

Table 2 Comparison of Systems

  Lab Trial New System Old System
Average 99.99 100.28 100.1
Std Dev 0.2 0.69 0.26

Success Rating:

A follow up test, usually based on company input.

Conclusion:

The new system yielded similar results as the current system.

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