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Trial Number 27

Trial Purpose:

To evaluate the effectiveness of SB-27 (t-Butyl Acetate 70% (CAS No: 540-88-5) + Benzyl Alcohol 30% (CAS No: 100-51-6)) and SB-32 (Ethyl Lactate 81% (CAS No: 97-64-3) + Propylene Carbonate 19% (CAS No: 108-32-7)) in removing greases from stainless steel coupons as a potential replacement of TCE with a heated ultrasonic cleaning method.

Date Run:

07/24/2024

Experiment Procedure:

Three stainless steel coupons were used for each cleaner and soil combination, making a total of twelve coupons. The initial weights of each coupon were recorded. Around 0.1 g of each contaminant was added to the bottom third of the coupon with a swab, and the dirty weights of each coupon were then recorded. The coupons were then subjected to heated ultrasonics in the cleaner for 15 minutes at a temperature of 120 °F. After the coupons were cleaned, they were left to air dry over night, and clean weights of each coupon were taken the following day.

Trial Results:

Cleaner Soil Initial weight of cont. Final weight of cont. % Content Removed Average % Removal
SB-27 DAW 330B 0.0761 0.0664 12.75 -21.63
0.0420 0.0550 -30.95
0.0863 0.1266 -46.70
Slide Gel No. 7 0.0523 0.0106 79.73 62.48
0.0407 0.0102 74.94
0.0476 0.0320 32.77
SB-32 DAW 330B 0.0188 0.0007 96.28 91.95
0.0254 0.0027 89.37
0.0286 0.0028 90.21
Slide Gel No. 7 0.0409 0.0087 78.73 83.02
0.0355 0.0066 81.41
0.0334 0.0037 88.92

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

Overall, the cleaners were not effective in removing the contaminants, but the only one that worked well enough was SB-32 on DAW 330B. When taking the coupons out of the cleaner, thick clumps of soil clung together and slipped right off the coupons. For the coupons in SB-27, the soil clung together the same way, but it was still attached to the coupon when I took them out, and they even seemed to absorb some of the cleaner and make the averages negative.

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