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Trial Number 5

Trial Purpose:

Test out the two new Oakite products

Date Run:

07/06/1995

Experiment Procedure:

The Inproclean #2000 is a no foaming version of the Inproclean #3800. The Inproclean 61B is a powdered aluminum and steel cleaner.
The Inproclean #2000 will be used at 10% by volume concentration while 20 grams of Inproclean 61B will be dissolved in 500 ml of water. Cleaning will take place at 150 F for 20 minutes. The coupons will then be rinsed for 2 minutes in 150 F tap water and dried under air knives for 2 minutes and dried in a convection oven set at 120 F for one hour.
Gravimetric analysis will be used to estimate the removal of all four contaminants. The coupons will be observed under a black light to notice any residual wax or quench oil. FTIR will be used to notice any non-visible traces of waxes or oils.

SUBSTRATE MATERIAL: #1- 6061 Aluminum coupons, #2- 110 Copper Coupons, #3- 260 Brass Coupons, #4 Carbon Steel pieces
CONTAMINANTS: #1- Wax, #2- Tap magic cutting fluid, #3- SafeTap grinding lubricant, #4- CI Hayes Quench Oil
CONTAMINATING PROCESS USED: coupons were dipped in wax and the oils were applied with a swab.

Trial Results:

Absolutely no foam, and very good wax and oil rejection. There was no etching on any of the coupons. As in all previous trials there is a slight bit of wax remaining on the coupons. Visually, all the oils were removed but a slight bit of Safetap was detected by the FTIR. Definitely need more mechanical energy to remove the wax residue. Increased air agitation with brushing should accomplish this.
Probably one of the best wax removers, but the Inproclean 61B foams up quite a bit and it etches the brass pretty bad, shouldn't be considered by Plating Job Shop.

EXPERIMENTAL DATA LOG

                                                    GRAVIMENTRIC ANALYSIS

Sample # and substrate clean mass (g) mass with contamination (g) mass after cleaning (g) contaminant removed (g) Percent Removal
#4-Al 20.9807 21.7228 21.0077 0.7151 96.36%
#10-Al 20.9982 21.7389 21.0008 0.7381 99.65%
#3545- Cu 35.3483 36.0925 35.3498 0.7427 99.80%
#4076- Cu 35.4014 36.2451 35.4019 0.8432 99.94%
#4687-Br 34.4644 35.2208 34.4650 0.7558 99.92%
#4080-Br 34.4050 35.1950 34.4066 0.7884 99.80%
#23-Steel 128.7159 129.8784 128.7243 1.1541 99.28%
#69-Steel 152.9184 154.2190 152.9235 1.2955 99.61%
#18-Al 21.0125 22.4750 21.0126 1.4624 99.99%
#26-Al 21.0039 22.3597 21.0040 1.3557 99.99%
#5581-Cu 35.5524 36.5757 35.5524 1.0233 100.00%
#4509-Cu 35.4532 36.2085 35.4527 0.7558 100.07%
#5054-Br 34.4965 35.4915 34.4968 0.9947 99.97%
#4459-Br 34.4373 35.3729 34.4364 0.9365 100.10%
#37-Steel 176.2809 178.4399 176.2828 2.1571 99.91%
#53-Steel 132.4426 133.8878 132.4431 1.4447 99.97%

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

The Oakite Inproclean #2000 is probably the most promising of the cleaners tested to date.  Need to further test for Plating Job Shop next week.

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