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Trial Number 3

Trial Purpose:

To test two solvents in cleaning oil and grease from stainless steel as an alternative to TCE using heated ultrasonics.

Date Run:

06/01/2023

Experiment Procedure:

Two solvents were identified previously using the Hspip software; SB-33 (D-limonene 85% +Dimethyl glutarate 15%) and SB-31 (Benzyl alcohol 63% + Ethyl lactate 37%).  Twelve stainless steel coupons were chosen and initial weights of each were recorded.  Half of the coupons were soiled with Hocut 795 and half were soiled with RI-780.  The soils were applied to the bottom third of each coupon using a swab.  The coupons were then cleaned by their respective solvent using a method of heated ultrasonics.  The coupons were immersed and subjected to ultrasonics agitation for 15 minutes at 130 degrees Farenheit.  The coupons were then removed and left to dry overnight.  (Coupons dried for a week before weights were taken). Clean weights were recorded.  

Trial Results:

Cleaner Soil Substrate Initial wt of cont. Final wt of cont. %Cont Removed % AVG % Overall
SB-33 1 Stainless Steel 0.0191 0.0038 80.10 88.20 0.88
Stainless Steel 0.0374 0.0040 89.30
Stainless Steel 0.0729 0.0035 95.20
2 Stainless Steel 0.0279 0.0012 95.70 87.63
Stainless Steel 0.0453 0.0042 90.73
Stainless Steel 0.0204 0.0048 76.47
SB-31 1 Stainless Steel 0.1060 0.0016 98.49 98.98 0.96
Stainless Steel 0.1202 0.0006 99.50
Stainless Steel 0.0662 0.0007 98.94
2 Stainless Steel 0.0284 0.0004 98.59 93.19
Stainless Steel 0.0123 0.0016 86.99
Stainless Steel 0.0100 0.0006 94.00

Coupons were left for a week after cleaning and were able to airdry during that time

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

SB-33 is an effective solvent in removing the soils from stainless steel coupons using heated ultrasonics.  SB-31 is an effective solvent in removing the soils from stainless steel coupons using heated ultrasonics.  

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