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Trial Number 18

Trial Purpose:

To evaluate the effectiveness of SB-2, SB-11, SB-22, SB-23, and SB-32 in removing Slide Gel No. 7 from copper and brass coupons as a potential replacement for TCE with an unheated ultrasonic cleaning method.

Date Run:

02/24/2024

Experiment Procedure:

Three copper and brass coupons were used for each cleaner being tested, for a total of 15 coupons per cleaner. The initial weights of each coupon were recorded. The bottom third of every coupon was soiled by applying the contaminate with a swab. The dirty weights of each coupon were then recorded. The coupons were then subjected to unheated ultrasonic in the cleaners for 15 minutes. After the coupons were cleaned, they were left to air-dry overnight. The next morning, the clean weights of each coupon were taken.

Trial Results:

Substrate Cleaner Coupon # Initial wt of cont. Final wt of cont. %Cont Removed Average % Removal
Copper SB-2 2 0.0619 0.0714 -15.35 -74.60
11 0.0269 0.0675 -150.93
16 0.0386 0.0608 -57.51
SB-11 16 0.0264 0.0312 -18.18 -12.06
26 0.0314 0.0298 5.10
40 0.0290 0.0357 -23.10
SB-22 7 0.0590 0.0124 78.98 82.10
17 0.0348 0.0022 93.68
39 0.0531 0.0140 73.63
SB-23 5 0.0305 0.0018 94.10 97.69
21 0.0529 0.0015 97.16
29 0.0390 -0.0007 101.79
SB-32 4 0.0329 0.0163 50.46 73.11
25 0.0276 0.0056 79.71
27 0.0406 0.0044 89.16
Brass SB-2 7 0.0384 0.0058 84.90 43.33
14 0.027 0.0299 -10.74
22 0.0326 0.0144 55.83
SB-11 11 0.0241 0.0175 27.39 26.07
18 0.0432 0.0177 59.03
32 0.0305 0.033 -8.20
SB-22 5 0.0355 0.0152 57.18 60.61
26 0.0412 0.0168 59.22
31 0.035 0.0121 65.43
SB-23 2 0.0425 0.0105 75.29 86.13
15 0.0309 0.0013 95.79
25 0.0244 0.0031 87.30
SB-32 6 0.0572 0.0173 69.76 63.89
10 0.0533 0.0222 58.35
28 0.0343 0.0125 63.56

Success Rating:

Preliminary compatibility tests on substrate coupons encouraging for at least one cleaning chemistry. More in-depth laboratory testing necessary.

Conclusion:

SB-2 and SB-11 did not dry properly overnight, making their final contents higher than their initials. SB-22 and SB-23 seemed like effective alternatives, but due to the "overcleaning" causing negative percent removals, further testing could be done to create the ideal range of cleaning time and contaminants added. SB-32 turned light blue after testing, this was caused by the Ethyl Lactate stripping copper ions from the metal and the mixture will not be used in further testing.

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