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Trial Number 0

Trial Purpose:

To identify a replacement to Trichloroethylene in cleaning buffing compounds from brass fixtures.

Date Run:

03/27/2000

Experiment Procedure:

Eight cleaners were selected based on the lab’s database of effective testing and Industrial Cleaning Survey: Directory of Vendors 4th edition. Seven of the chemistries were diluted to 5% in 600 ml beakers using DI water. These seven were then heated to 130 F on a hot plate. The final cleaner was used at full strength and room temperature. Twenty-four preweighed brass coupons were contaminated with the buffing compound and weighed again. Three coupons were cleaned in one solution for five minutes using stir-bar agitation. Coupons were rinsed in tap water at 120 F for 30 seconds and dried using a Master Appliance Corp, Hot-air gun model HG-301A at 500 F for one minute. After coupons returned to room temperature, final clean weights were recorded and the percent efficiency was calculated.

SUBSTRATE MATERIAL: Brass Coupons
CONTAMINANTS: Jackson Lea, Antique Buffing Compound LM-12 (CAS#s:9000-70-8,1344-28-1,409-21-2,1309-37-1)

Trial Results:

US Polychem Polyspray 790 P was the only cleaner to remove all of the buffing compound from the brass coupons. Oakite Inproclean 3800 removed nearly 85% of the contaminant. WR Grace Daraclean 282 GF and International Products Micro 90 both had efficiencies over 70%. Table 1 lists all of the calculated cleaning efficiencies.

Table 1. Cleaning Efficiencies

Chemistry Pressure Wash Micro 90 Gillite 160 X Inproclean Dirtex Polyspray Daraclean Engine Degreaser
Coupon 1 30.53 67.35 44.16 89.41 80.96 100.80 75.00 45.99
Coupon 2 31.24 87.73 40.21 90.48 71.83 100.47 71.92 76.39
Coupon 3 16.44 60.19 41.02 73.19 55.11 100.48 72.46 56.65
Average 26.07 71.76 41.80 84.36 69.30 100.58 73.13 59.68

Success Rating:

Results successful using TACT (time, agitation, concentration, and temperature, as well as rinsing and drying) and/or other cleaning chemistries examined.

Conclusion:

The four products that removed over 70% of the buffing compound will be further tested using the second supplied buffing compound.  Additional testing will be performed on the supplied parts as well.

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